Sunday, 11 September 2016

PHYTOCHEMICAL AND PROXIMATE ANALYSIS OF Azadirachta indica BARK AND LEAF



ABSTRACT
The proximate and phytochemical analysis of Azadirachta indica was investigated. The bark and the leaves were first extracted by using both aqueous and ethanol solutions. Proximate analysis showed the leaves to contain 84.50  0.1 Moisture, 2.52  0.02 Ash, 4.61 0.01 Protein, 0.062  0.02 Fat, 2.64 0.01 Fibre, 89.53  0.02 Carbohydrate, while the bark contained 49.50  Moisture, 7.10  0.1 Ash, 3.30  0.1 Protein, 0.81  0.01 Fat, 6.65  0.02 Fiber and 81.9  0.01 Carbohydrate. Phytochemical screening showed very strong presence of Alkaloids, Glycosides, Flavonoids, Reducing compounds and Polyphenol in both aqueous and ethanol extract of the leaves while the bark showed appreciable presence of Alkaloids, Reducing compounds and Polyphenol in both aqueous and ethanol extracts. Tannins, Phlobatanin Anthraquinones and Hydroxymethyl anthraquinones are absent in the bark of the plant while the leaves do not contain Phlobatanin, Anthraquinones, Hydroxymethyl anthraquinones in both aqueous and ethanol extracts. Saponins were also discovered to be absent in ethanol extracts of both the leaves and bark of the plant. It is discovered that these compounds are present in both the leaves and the bark hence their combined use in traditional remedies with same therapeutics effects in treatment of malaria and other ailments.


TABLE OF CONTENTS
Title page  -        -        -        -        -        -        -        -        -        i
Certification        -        -        -        -        -        -        -        -        ii
Dedication -        -        -        -        -        -        -        -        -        iii
Acknowledgements       -        -        -        -        -        -        -        iv
Abstract    -        -        -        -        -        -        -        -        -        v
Table of contents -        -        -        -        -        -        -        -        vi
List of tables       -        -        -        -        -        -        -        -        ix
CHAPTER ONE: INTRODUCTION
1.1                     Background of the study    -        -        -        -        -        1
1.2                     Description and uses of Azadirachta indica.   -        -        4
1.3                     Justification     -        -        -        -        -        -        -        7
1.4                     Aims and objectives. -        -        -        -        -        -        8
CHAPTER TWO: LITERATURE REVIEW
2.1        Pharmacological importance of phytochemical                           
compounds in plants -        -        -        -        -        -        9
    
2.1.2       Flavonoids     -        -        -        -        -        -        -        11
2.1.3     Alkaloids         -        -        -        -        -        -        -        12
2.1.4     Saponins         -        -        -        -        -        -        -        -        14
2.1.5     Tannins  -        -        -        -        -        -        -        -        15
2.1.6     Digitalis glycosides   -        -        -        -        -        -        17
2.2        Proximate composition of plants -        -        -        -        19
CHAPTER THREE: MATERIALS AND METHOD
3.1        Collection and identification of plant materials        -        -        22
3.2        Preparation of plant materials     -        -        -        -        22    
3.2.1     Preparation of alcoholic plant extract    -        -        -        22  
3.2.2     Preparation of aqueous plant extract     -        -        -        23 
3.3        Experimental procedures    -        -        -        -        -        23
3.3.1     Test for alkaloids (Sofowora, 1993)      -        -        -        23
3.3.2     Test for glycosides (Sofowora, 1993)    -        -        -        23

3.3.3     Test for tannins (Trease and Evans, 1989)               -        24 
3.3.4     Test for saponins (Sofowora, 1984) Frothing test    -        24
3.3.5     Test for flavonoids (Guilei, 1982)          -        -        -        -        24  
3.3.6     Test for reducing sugar (Guilei, 1982) Fehling’s test          -        25   
3.3.7     Test for polyphenol (Guilei, 1982)        -        -        -        -        25
3.3.8     Test for phlobatanin (Trease and Evans, 1982)       -        -        25
3.3.9      Test for anthraquinones (Trease and Evans, 1982) -        25   
3.3.10    Test for hydroxymethyl anthraquinones (Guilei, 1988)    26
3.4         Proximate composition analysis -        -        -        -        26
3.4.1      Carbohydrate content (A. O. A. C., 1990)     -        -        26    
3.4.2      Crude protein (A. O. A. C., 1990)        -        -        -        -        26       
3.4.3      Crude fat (A. O. A. C., 1990)     -        -        -        -        27     
3.4.4     Crude fibre (A. O. A. C., 1990)   -        -        -        -        27
3.4.5      Ash content (A. O. A. C., 1990) -        -        -        -        28  
3.4.6      Moisture content (A. O. A. C., 1990)   -        -        -        28
CHAPTER FOUR: RESULTS AND DISCUSSION
4.1         Results  -        -        -        -        -        -        -        -        29
4.1.1       Phytochemical screening of Azadirachta indica       -        -        29

4.1.2      Proximate composition of bark and leaves of
              Azadirachta indica   -        -        -        -        -        -        29

4.2         Discussion of findings       -        -        -        -        -        35
CHAPTER FIVE: SUMMARY, CONCLUSION AND RECOMMENDATIONS

5.1   Summary and conclusion        -        -        -        -        -        -        37
5.2   Recommendations         -        -        -        -        -        -        -        38 
REFERENCES    -        -        -        -        -        -        -        39
APPENDICES     -        -        -        -        -        -        -        45


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